Title : ( Synthesis and Crystal Structure of 5,5-Dimethyl-2-(p-methylanilino)-2-oxo-1,3,2-diazaphosphorinane )
Authors: Khodayar Gholivand , Mehrdad Pourayoubi , Sedigheh Farshadian , Soheila Molani , Zahra Shariatinia ,Abstract
The crystal Structure of 5,5-dimethyl-2-(p-methylanilino)-2-oxo-1,3,2-diazaphosphorinane has been determined. The P-N bond lengths are significantly shorter than the P-N single bond. The P=O bond is placed in an equatorial position and is slightly longer than the PO double bond length. The molecule is obtained in the form of a two dimensional polymer via intermolecular -N-H...O=P- and -N-H...N- hydrogen bonds. A weak C-H...O hydrogen bond is also observed in the structure.
Keywords
, Synthesis and Crystal Structure of 5, 5-Dimethyl-2-(p-methylanilino)-2-oxo-1, 3, 2-diazaphosphorinane@article{paperid:1011634,
author = {Khodayar Gholivand and Pourayoubi, Mehrdad and Sedigheh Farshadian and Soheila Molani and Zahra Shariatinia},
title = {Synthesis and Crystal Structure of 5,5-Dimethyl-2-(p-methylanilino)-2-oxo-1,3,2-diazaphosphorinane},
journal = {X-ray Structure Analysis Online},
year = {2005},
volume = {21},
number = {3},
month = {March},
issn = {1883-3578},
pages = {55--56},
numpages = {1},
keywords = {Synthesis and Crystal Structure of 5;5-Dimethyl-2-(p-methylanilino)-2-oxo-1;3;2-diazaphosphorinane},
}
%0 Journal Article
%T Synthesis and Crystal Structure of 5,5-Dimethyl-2-(p-methylanilino)-2-oxo-1,3,2-diazaphosphorinane
%A Khodayar Gholivand
%A Pourayoubi, Mehrdad
%A Sedigheh Farshadian
%A Soheila Molani
%A Zahra Shariatinia
%J X-ray Structure Analysis Online
%@ 1883-3578
%D 2005