Title : ( N,N -Di-tert-butyl-N -(2,6-difluoro-benzoyl) phosphoric triamide )
Authors: Mehrdad Pourayoubi , Atekeh Tarahhomi , Arnold L. Rheingold , James A. Golen ,
Full TextAbstract
In the title compound, C15H24F2N3O2P, the phosphoryl and carbonyl groups adopt anti positions relative to each other. The P atom is in a tetrahedral coordination environment and the environment of each N atom is essentially planar. In the crystal, adjacent molecules are linked via N—H...O P and N—H...O C hydrogen bonds into an extended chain parallel to the a axis. The crystal studied was a nonmerohedral twin with a minor twin component of 36.4 (1)%.
Keywords
, single, crystal X, ray study; T = 200 K; mean (C–C) = 0.005 A°; R factor = 0.049; wR factor = 0.121; data, to, parameter ratio = 18.9.
@article{paperid:1018508,
author = {Pourayoubi, Mehrdad and Tarahhomi, Atekeh and Arnold L. Rheingold and James A. Golen},
title = {N,N -Di-tert-butyl-N -(2,6-difluoro-benzoyl) phosphoric triamide},
journal = {Acta Crystallographica Section E: Structure Reports Online},
year = {2010},
volume = {66},
number = {12},
month = {December},
issn = {1600-5368},
pages = {3159--3159},
numpages = {0},
keywords = {single-crystal X-ray study; T = 200 K; mean (C–C) = 0.005 A°;
R factor = 0.049; wR factor = 0.121; data-to-parameter ratio = 18.9.},
}
%0 Journal Article
%T N,N -Di-tert-butyl-N -(2,6-difluoro-benzoyl) phosphoric triamide
%A Pourayoubi, Mehrdad
%A Tarahhomi, Atekeh
%A Arnold L. Rheingold
%A James A. Golen
%J Acta Crystallographica Section E: Structure Reports Online
%@ 1600-5368
%D 2010
