Title : ( N-Cyclohexylcyclohexanaminium chloride )
Authors: Mehrdad Pourayoubi , monireh negari , Marek Necas ,
Full TextAbstract
In the title salt, C12H24N+Cl , both cyclohexyl rings adopt chair conformations and the NH2 unit is situated in the equatorial position with respect to the rings in the cation. The large C—N—C bond angle [117.99 (14)] in the cation is a result of linking two bulky cyclohexyl rings to the N atom. The aminium H atoms are involved in intermolecular N—H...Cl hydrogen bonds, forming an infinite zigzag chain parallel to the c axis. The crystal studied was a racemic twin with a twin fraction of 0.28 (18).
Keywords
, single, crystal X, ray study; T = 120 K; mean (C–C) = 0.003 A° ; R factor = 0.025; wR factor = 0.057; data, to, parameter ratio = 9.0.
@article{paperid:1019262,
author = {Pourayoubi, Mehrdad and Negari, Monireh and Marek Necas},
title = {N-Cyclohexylcyclohexanaminium chloride},
journal = {Acta Crystallographica Section E: Structure Reports Online},
year = {2011},
volume = {67},
number = {2},
month = {February},
issn = {1600-5368},
keywords = {single-crystal X-ray study; T = 120 K; mean (C–C) = 0.003 A°
;
R factor = 0.025; wR factor = 0.057; data-to-parameter ratio = 9.0.},
}
%0 Journal Article
%T N-Cyclohexylcyclohexanaminium chloride
%A Pourayoubi, Mehrdad
%A Negari, Monireh
%A Marek Necas
%J Acta Crystallographica Section E: Structure Reports Online
%@ 1600-5368
%D 2011
