Acta Crystallographica Section E: Structure Reports Online, ( ISI ), Volume (67), No (8), Year (2011-8) , Pages (2202-2202)

Title : ( Phenyl bis(morpholin-4-ylamido)-phosphinate )

Authors: Mehrdad Pourayoubi , Hossein Eshtiagh Hosseini , monireh negari , Marek Nečas ,

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In the title compound, C14H23N4O4P, the P atom is in a distorted tetrahedral environment with bond angles in the range 96.87 (6)–119.86 (6)°. The two morpholinyl groups adopt a chair conformation. The phenyl ring is disordered over two sets of sites with equal occupancies [0.500 (2)]. In the crystal, adjacent molecules are linked via N—H...O hydrogen bonds into an extended chain running parallel to the a axis. Only one of the amidate N—H groups is involved in hydrogen bonding.

Keywords

, single, crystal X, ray study; T = 120 K; mean _(C–C) = 0.002 Å; disorder in main residue; R factor = 0.029; wR factor = 0.070; data, to, parameter ratio =
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@article{paperid:1023911,
author = {Pourayoubi, Mehrdad and Eshtiagh Hosseini, Hossein and Negari, Monireh and Marek Nečas},
title = {Phenyl bis(morpholin-4-ylamido)-phosphinate},
journal = {Acta Crystallographica Section E: Structure Reports Online},
year = {2011},
volume = {67},
number = {8},
month = {August},
issn = {1600-5368},
pages = {2202--2202},
numpages = {0},
keywords = {single-crystal X-ray study; T = 120 K; mean _(C–C) = 0.002 Å; disorder in main residue; R factor = 0.029; wR factor = 0.070; data-to-parameter ratio = 11.0.},
}

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%0 Journal Article
%T Phenyl bis(morpholin-4-ylamido)-phosphinate
%A Pourayoubi, Mehrdad
%A Eshtiagh Hosseini, Hossein
%A Negari, Monireh
%A Marek Nečas
%J Acta Crystallographica Section E: Structure Reports Online
%@ 1600-5368
%D 2011

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