Title : ( N,N -Bis(2-methylphenyl)-N -(2,2,2- trichloroacetyl)phosphoric triamide )
Authors: Mehrdad Pourayoubi , MOJTABA KEIKHA , Masood Parvez ,
Full TextAbstract
In the title compound, C16H17Cl3N3O2P, the P—N bonds in the P(O)[NH(2—CH3)C6H4]2 unit [1.623 (4) and 1.637 (3) Å] are shorter than the P—N bond in the C(O)NHP(O) fragment [1.704 (3) Å]. The phosphoryl and carbonyl groups are anti with respect to each other and the P atom has a distorted tetrahedral configuration. In the crystal, adjacent molecules are linked via N—H…O(P) and N—H…O(C) hydrogen bonds into an extended chain parallel to [101].
Keywords
, single, crystal X, ray study; T = 173 K; mean σ(C–C) = 0.007 Å; R factor = 0.071; wR factor = 0.141; data, to, parameter ratio = 18.8
@article{paperid:1023917,
author = {Pourayoubi, Mehrdad and KEIKHA, MOJTABA and Masood Parvez},
title = {N,N -Bis(2-methylphenyl)-N -(2,2,2- trichloroacetyl)phosphoric triamide},
journal = {Acta Crystallographica Section E: Structure Reports Online},
year = {2011},
volume = {67},
number = {10},
month = {October},
issn = {1600-5368},
pages = {2792--2792},
numpages = {0},
keywords = {single-crystal X-ray study; T = 173 K; mean σ(C–C) = 0.007 Å; R factor = 0.071; wR factor = 0.141; data-to-parameter ratio = 18.8},
}
%0 Journal Article
%T N,N -Bis(2-methylphenyl)-N -(2,2,2- trichloroacetyl)phosphoric triamide
%A Pourayoubi, Mehrdad
%A KEIKHA, MOJTABA
%A Masood Parvez
%J Acta Crystallographica Section E: Structure Reports Online
%@ 1600-5368
%D 2011
