Title : ( Cyclohexyl(methyl)ammonium(bis[cyclohexyl(methyl)amino]-phosphoryl)(4-methylphenylsulfonyl)-azanide )
Authors: Mehrdad Pourayoubi , hassan fadaei , Atekeh Tarahhomi , Masood Parvez ,Abstract
In the anion of the title salt, C7H16N+.C21H35N3O3PS-, the P and S atoms are both in distorted tetrahedral environments and the angles at the tertiary N atoms confirm their sp2 character. The two S=O groups are in syn and gauche conformations with respect to the phosphoryl group. In the crystal, N—H…O(=S) and N—H…O(=P) hydrogen bonds involving two anions and two cations form a centrosymmetric four-component cluster.
Keywords
, single, crystal X, ray study; T = 173 K; mean σ(C–C) = 0.007 Å; R factor = 0.085; wR factor = 0.189; data, to, parameter ratio = 21.9@article{paperid:1023999,
author = {Pourayoubi, Mehrdad and Fadaei, Hassan and Tarahhomi, Atekeh and Masood Parvez},
title = {Cyclohexyl(methyl)ammonium(bis[cyclohexyl(methyl)amino]-phosphoryl)(4-methylphenylsulfonyl)-azanide},
journal = {Acta Crystallographica Section E: Structure Reports Online},
year = {2011},
volume = {67},
number = {10},
month = {October},
issn = {1600-5368},
pages = {2795--2795},
numpages = {0},
keywords = {single-crystal X-ray study; T = 173 K; mean σ(C–C) = 0.007 Å; R factor = 0.085; wR factor = 0.189; data-to-parameter ratio = 21.9},
}
%0 Journal Article
%T Cyclohexyl(methyl)ammonium(bis[cyclohexyl(methyl)amino]-phosphoryl)(4-methylphenylsulfonyl)-azanide
%A Pourayoubi, Mehrdad
%A Fadaei, Hassan
%A Tarahhomi, Atekeh
%A Masood Parvez
%J Acta Crystallographica Section E: Structure Reports Online
%@ 1600-5368
%D 2011