Title : ( 2Aminopyridinium bis(pyridine-2,6-dicarboxylato)ferrate-III )
Authors: Masoud Mirzaei Shahrabi , Hossein Eshtiagh Hosseini , Joel T. Mague ,
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Abstract
In the title compound, (C5H7N2)[Fe(C7H3NO4)2] or [2-apyH]- [Fe(pydc)2], the asymmetric unit contains an [Fe(pydc)2] (pydc is pyridine-2,6-dicarboxylate) anion and a protonated 2- aminopyridine cation ([2-apyH]+). The complex anion contains an FeIII atom within a distorted octahedral FeN2O4 coordination geometry. N—H O and C—H O hydrogen bonding, offset – stacking [centroid–centroid distance = 3.805 (13) A ˚ ] and C O interactions [3.494 (14) A ˚ ] generate a three-dimensional network structure.
Keywords
, single, crystal X, ray study; T = 100 K; mean (C–C) = 0.002 A° ; R factor = 0.033; wR factor = 0.086; data, to, parameter ratio = 16.6.
@article{paperid:1025603,
author = {Mirzaei Shahrabi, Masoud and Eshtiagh Hosseini, Hossein and Joel T. Mague},
title = {2Aminopyridinium bis(pyridine-2,6-dicarboxylato)ferrate-III},
journal = {Acta Crystallographica Section E: Structure Reports Online},
year = {2012},
volume = {68},
number = {68},
month = {January},
issn = {1600-5368},
pages = {174--174},
numpages = {0},
keywords = {single-crystal X-ray study; T = 100 K; mean (C–C) = 0.002 A°
;
R factor = 0.033; wR factor = 0.086; data-to-parameter ratio = 16.6.},
}
%0 Journal Article
%T 2Aminopyridinium bis(pyridine-2,6-dicarboxylato)ferrate-III
%A Mirzaei Shahrabi, Masoud
%A Eshtiagh Hosseini, Hossein
%A Joel T. Mague
%J Acta Crystallographica Section E: Structure Reports Online
%@ 1600-5368
%D 2012
