Title : ( O,O- -Dimethyl (cyclohexylamido)thio- phosphate )
Authors: Fahimeh Sabbaghi , Mehrdad Pourayoubi , Marek Nečas ,
Full TextAbstract
The P atom in the title compound, C8H18NO2PS, is bonded in a distorted tetrahedral PSO2N environment with bond angles in the range of 99.23 (5)–115.17 (4)°. The cyclohexane ring is disordered over two sets of sites with refined occupancies of 0.528 (5) and 0.472 (5). The ring in both disorder components adopts a chair conformation with the N—H group oriented equatorially. In the crystal, pairs of P═S…H—N hydrogen bonds form inversion dimers.
Keywords
, single, crystal X, ray study; T = 120 K; mean σ(O–C) = 0.002 Å; disorder in main residue; R factor = 0.025; wR factor = 0.069; data, to, parameter ratio = 11.9.
@article{paperid:1030649,
author = {Fahimeh Sabbaghi and Pourayoubi, Mehrdad and Marek Nečas},
title = {O,O- -Dimethyl (cyclohexylamido)thio- phosphate},
journal = {Acta Crystallographica Section E: Structure Reports Online},
year = {2012},
volume = {68},
number = {10},
month = {October},
issn = {1600-5368},
pages = {2891--2891},
numpages = {0},
keywords = {single-crystal X-ray study; T = 120 K; mean σ(O–C) = 0.002 Å; disorder in main residue; R factor = 0.025; wR factor = 0.069; data-to-parameter ratio = 11.9.},
}
%0 Journal Article
%T O,O- -Dimethyl (cyclohexylamido)thio- phosphate
%A Fahimeh Sabbaghi
%A Pourayoubi, Mehrdad
%A Marek Nečas
%J Acta Crystallographica Section E: Structure Reports Online
%@ 1600-5368
%D 2012
