Title : ( Diphenyl (isopropylamido) phosphate )
Authors: Fahimeh Sabbaghi , Mehrdad Pourayoubi , Marek Nečas , Michal Babiak ,
Full TextAbstract
The P atom in the title compound, C15H18NO3P, is in a distorted tetrahedral P(O)(O)2N environment; the bond angles at P are in the range 98.16 (6)–115.82 (6)°. In the crystal, adjacent molecules are linked via N—H…O═P hydrogen bonds into a chain running parallel to the b axis. The methyl groups are disordered over two sets of sites in a 0.677 (14):0.323 (14) ratio. The crystal studied was a nonmerohedral twin with a refined minor component of 22.31 (4)%.
Keywords
, single, crystal X, ray study; T = 120 K; mean σ(C–C) = 0.003 Å; disorder in main residue; R factor = 0.027; wR factor = 0.081; data, to, parameter ratio = 29.9.
@article{paperid:1031379,
author = {Fahimeh Sabbaghi and Pourayoubi, Mehrdad and Marek Nečas and Michal Babiak},
title = {Diphenyl (isopropylamido) phosphate},
journal = {Acta Crystallographica Section E: Structure Reports Online},
year = {2012},
volume = {68},
number = {12},
month = {December},
issn = {1600-5368},
pages = {3459--3459},
numpages = {0},
keywords = {single-crystal X-ray study; T = 120 K; mean σ(C–C) = 0.003 Å; disorder in main residue; R factor = 0.027; wR factor = 0.081; data-to-parameter ratio = 29.9.},
}
%0 Journal Article
%T Diphenyl (isopropylamido) phosphate
%A Fahimeh Sabbaghi
%A Pourayoubi, Mehrdad
%A Marek Nečas
%A Michal Babiak
%J Acta Crystallographica Section E: Structure Reports Online
%@ 1600-5368
%D 2012
