Journal of the American Ceramic Society, ( ISI ), Volume (92), No (5), Year (2009-5) , Pages (990-995)

Title : ( The Effect of Conformation Method and Sintering Technique on the Densification and Grain Growth of Nanocrystalline 8 mol% Yttria‐Stabilized Zirconia )

Authors: Mehdi Mazaheri , Z. Razavi Hesabi , F. Golestani-Fard , Sahar Mollazadeh Beidokhti , S. Jafari , S. K. Sadrnezhaad ,

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Abstract

Uniaxial dry pressing (DP) and slip casting (SC) were used to form green bodies of nanocrystalline 8 mol% yttria-stabilized zirconia powder processed via the glycine-nitrate combustion method. The SC method was shown to be a more efficient, yielding more homogenous green bodies with higher green density (60% theoretical density) which contained smaller pores with narrower distribution. Improved green properties resulted in lowering the sintering temperature of SC bodies by about 2001C compared with DP compacts. Consequently, the grain growth in sintered bodies formed by SC was relatively abated. By taking the benefits of the wet conformation method, the final grain size of nearly full dense (497% TD) structures was reduced by 39% (i.e. from 2.15 to 1.3lm). To reveal the effect of sintering technique, DP bodies were sintered via both microwave and two-step sintering methods. While the grain size of two-step sintered samples waso300 nm, sintering via microwave radiation yielded a nearly full dense structure with a mean grain size of 0.9lm. The results show that conventionally sintered SC bodies posses higher indentation fracture toughness (FT) (B3 MPa.m 1/2 ) compared with DP samples (1.6 MPa .m 1/2 ). Interestingly, it was shown that, without applying any modified sintering technique, the hardness and FT of SC bodies with coarser structures are completely close to those of samples sintered via microwave heating.

Keywords

, Sintering process, Zirconia Densification and Grain Growth
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@article{paperid:1038360,
author = {Mehdi Mazaheri and Z. Razavi Hesabi and F. Golestani-Fard and Mollazadeh Beidokhti, Sahar and S. Jafari and S. K. Sadrnezhaad},
title = {The Effect of Conformation Method and Sintering Technique on the Densification and Grain Growth of Nanocrystalline 8 mol% Yttria‐Stabilized Zirconia},
journal = {Journal of the American Ceramic Society},
year = {2009},
volume = {92},
number = {5},
month = {May},
issn = {0002-7820},
pages = {990--995},
numpages = {5},
keywords = {Sintering process; Zirconia Densification and Grain Growth},
}

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%0 Journal Article
%T The Effect of Conformation Method and Sintering Technique on the Densification and Grain Growth of Nanocrystalline 8 mol% Yttria‐Stabilized Zirconia
%A Mehdi Mazaheri
%A Z. Razavi Hesabi
%A F. Golestani-Fard
%A Mollazadeh Beidokhti, Sahar
%A S. Jafari
%A S. K. Sadrnezhaad
%J Journal of the American Ceramic Society
%@ 0002-7820
%D 2009

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