Title : ( A facile hydrothermal synthesis of novel hollow triple-shell CuNiFe2O4 nanospheres with robust catalytic performance in the Suzuki–Miyaura coupling reaction )
Authors: maryam rajabzadeh , Reza Khalifeh , Hossein Eshghi , Mehdi Bakavoli ,
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Abstract
Triple-shell hollow spheres of crystalline copper–nickel ferrite have been synthesized in a simple one-pot procedure using carbon spheres as templates via a hydrothermal approach. Ferric nitrate, copper nitrate, and nickel nitrate were dissolved in water together with glucose, and the mixture was heated to 180 0C in an autoclave. Finally, the carbon core was removed by calcination at 550 0C. The triple-shell hollow spheres of CuNiFe2O4 were characterized by XRD, TEM, FE-SEM, and EDS. High catalytic activity for the Suzuki reaction was obtained for this new triple-shell hollow sphere of CuNiFe2O4. This also reveals obvious advantages such as the recyclability of the catalyst, simple experimental operation, and excellent yields.
Keywords
, Heterogeneous catalyst, Suzuki–Miyaura reaction, Micro/nanostructure, Hollow triple-shell nanospheres CuNiFe2O4
@article{paperid:1067592,
author = {Rajabzadeh, Maryam and Reza Khalifeh and Eshghi, Hossein and Bakavoli, Mehdi},
title = {A facile hydrothermal synthesis of novel hollow triple-shell CuNiFe2O4 nanospheres with robust catalytic performance in the Suzuki–Miyaura coupling reaction},
journal = {Journal of Catalysis},
year = {2018},
volume = {360},
number = {1},
month = {April},
issn = {0021-9517},
pages = {261--269},
numpages = {8},
keywords = {Heterogeneous catalyst; Suzuki–Miyaura reaction; Micro/nanostructure; Hollow triple-shell nanospheres
CuNiFe2O4},
}
%0 Journal Article
%T A facile hydrothermal synthesis of novel hollow triple-shell CuNiFe2O4 nanospheres with robust catalytic performance in the Suzuki–Miyaura coupling reaction
%A Rajabzadeh, Maryam
%A Reza Khalifeh
%A Eshghi, Hossein
%A Bakavoli, Mehdi
%J Journal of Catalysis
%@ 0021-9517
%D 2018
