ChemistrySelect, Volume (5), No (21), Year (2020-6) , Pages (6440-6452)

Title : ( An Eco‐Friendly and Efficient Approach for the Synthesis of Tetrazoles via Fe 3 O 4 /HT‐GLYMO‐TA as a New Recoverable Heterogeneous Nanostructured Catalyst )

Authors: maryam sadat ghasemzadeh , Batool Akhlaghinia ,

Citation: BibTeX | EndNote

Abstract

Tannic acid immobilized on functionalized magnetic hydrotalcite (Fe3O4/HT-GLYMO-TA) was synthesized as a durable, environmentally-friendly and magnetic nanostructured catalyst for the synthesis of 5- and 1-substituted-1H-tetrazoles. The nanocatalyst was characterized by several methods, Fourier transform infrared (FT-IR), X-ray diffraction (XRD) analysis, transmission electron microscopy (TEM), field emission scanning electron microscopy (FE-SEM), energy-dispersive X-ray spectroscopy (EDS), EDS-map, thermogravimetric analysis (TGA), vibrating sample magnetometry (VSM) and CHNS analysis. The results displayed that the superparamagnetic catalyst with a mean particle size of approximately 23–27 nm has a plate-like shape. The catalytic activity of this new nanostructured catalyst resulted in the preparation of tetrazoles with high yields. Additionally, this novel procedure offers a plethora of benefits including short reaction times, the simplicity of operation, the ease of purification procedure and the reusability of nanocatalyst for at least eight cycles.

Keywords

, green chemistry, heterogeneous catalysis, tannic acid, tetrazole
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@article{paperid:1080181,
author = {Ghasemzadeh, Maryam Sadat and Akhlaghinia, Batool},
title = {An Eco‐Friendly and Efficient Approach for the Synthesis of Tetrazoles via Fe 3 O 4 /HT‐GLYMO‐TA as a New Recoverable Heterogeneous Nanostructured Catalyst},
journal = {ChemistrySelect},
year = {2020},
volume = {5},
number = {21},
month = {June},
issn = {2365-6549},
pages = {6440--6452},
numpages = {12},
keywords = {green chemistry; heterogeneous catalysis; tannic acid; tetrazole},
}

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%0 Journal Article
%T An Eco‐Friendly and Efficient Approach for the Synthesis of Tetrazoles via Fe 3 O 4 /HT‐GLYMO‐TA as a New Recoverable Heterogeneous Nanostructured Catalyst
%A Ghasemzadeh, Maryam Sadat
%A Akhlaghinia, Batool
%J ChemistrySelect
%@ 2365-6549
%D 2020

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