Title : ( A redetermination of the structure and Hirshfeld surface analysis of catena-[(diaqua)di(μ-hydroxido)bis(μ-nicotinato-N-oxide)bis(μ-nicotinato-N-oxido)tricopper(II)] )
Authors: Masoud Mirzaei Shahrabi , Maryam Bazargan , POURIA EBTEHAJ , Joel T. Mague ,
Full TextAbstract
The product obtained from the reaction of pyridine-2,3-dicarboxylic acid and hydrated copper(II) chloride in hot aqueous NaOH solution was determined by low temperature X-ray diffraction to be {[Cu3(µ-OH)2(H2O)2(µ-nicNO)4]}n (nicNO is pyridine-3-carboxylate N-oxide), a structure obtained from room temperature data and previously reported. The present determination is improved in quality and treatment of the hydrogen atoms. A Hirshfeld surface analysis of the intermolecular interactions is presented
Keywords
, crystal structure; nicotinic acid N, oxide; copper; hydrogen bond
@article{paperid:1083490,
author = {Mirzaei Shahrabi, Masoud and Bazargan, Maryam and EBTEHAJ, POURIA and Joel T. Mague},
title = {A redetermination of the structure and Hirshfeld surface analysis of catena-[(diaqua)di(μ-hydroxido)bis(μ-nicotinato-N-oxide)bis(μ-nicotinato-N-oxido)tricopper(II)]},
journal = {Acta Crystallographica Section E: Crystallographic Communications},
year = {2021},
volume = {77},
number = {3},
month = {March},
issn = {2056-9890},
pages = {309--313},
numpages = {4},
keywords = {crystal structure; nicotinic acid N-oxide; copper; hydrogen bond},
}
%0 Journal Article
%T A redetermination of the structure and Hirshfeld surface analysis of catena-[(diaqua)di(μ-hydroxido)bis(μ-nicotinato-N-oxide)bis(μ-nicotinato-N-oxido)tricopper(II)]
%A Mirzaei Shahrabi, Masoud
%A Bazargan, Maryam
%A EBTEHAJ, POURIA
%A Joel T. Mague
%J Acta Crystallographica Section E: Crystallographic Communications
%@ 2056-9890
%D 2021
