9th International Seminar on Polymer Science and Technology , 2009-10-17

Title : ( Preparation of imide-siloxane/silica nanocomposite membrane )

Authors: maryam aldaghi , Ali Ahmadpour , Seyed Mojtaba Zebarjad , Majid Pakizeh ,

Citation: BibTeX | EndNote

Abstract

In this work, supported polyimide-siloxane hybrid membranes containing different percentages of silica were successfully prepared from pyromellitic dianhydride (PMDA), aminopropyltrimethoxysilane (APrTMOS) and tetramethoxysilane (TMOS) by polycondensation, imidisation and sol-gel reaction. Membranes were coated on supports by spin coating method and the film thickness was 1-3μm. The molecular structure and thermal performance of these membranes were characterized by using Fourier transform-infrared spectrometry (FT-IR) and thermogravimetric analysis (TGA). Scanning electron microscopy (SEM) was used to study the quality of coatings. The results indicated the presence of imide and Si-O-Si bonds in the sample. Weight loss of the hybrid polyimide membrane was reduced 29% compared to the pure polyimide. No defects or cracks were observed on the substrate/coating interface.

Keywords

, Polyimide, Silica, Nanocomposite, Membrane, spin coating
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@inproceedings{paperid:1014080,
author = {Aldaghi, Maryam and Ahmadpour, Ali and Zebarjad, Seyed Mojtaba and Pakizeh, Majid},
title = {Preparation of imide-siloxane/silica nanocomposite membrane},
booktitle = {9th International Seminar on Polymer Science and Technology},
year = {2009},
location = {IRAN},
keywords = {Polyimide-Silica-Nanocomposite-Membrane-spin coating},
}

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%0 Conference Proceedings
%T Preparation of imide-siloxane/silica nanocomposite membrane
%A Aldaghi, Maryam
%A Ahmadpour, Ali
%A Zebarjad, Seyed Mojtaba
%A Pakizeh, Majid
%J 9th International Seminar on Polymer Science and Technology
%D 2009

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