Title : ( N,N- -Dibenzyl-N-- -(2-chloro-2,2- difluoroacetyl)phosphoric triamide )
Authors: Mehrdad Pourayoubi , MOJTABA KEIKHA , Jerry P. Jasinski , Amanda C. Keeley ,
Full TextAbstract
In the title molecule, C16H17ClF2N3O2P, the N—H unit of the C(═O)NHP(═O) fragment adopts a syn orientation with respect to the P═O group. The two F atoms and the Cl atom of the ClF2C group are disordered over two sets of sites with refined occupancies of 0.605 (6) and 0.395 (6). In the crystal, molecules are linked via N—H…O═C hydrogen bonds and the (N—H…)(N—H…)O═P group into chains along [010].
Keywords
, single, crystal X, ray study; T = 173 K; mean σ(C–C) = 0.005 Å; disorder in main residue; R factor = 0.051; wR factor = 0.122; data, to, parameter ratio = 20.8.
@article{paperid:1030651,
author = {Pourayoubi, Mehrdad and KEIKHA, MOJTABA and Jerry P. Jasinski and Amanda C. Keeley},
title = {N,N- -Dibenzyl-N-- -(2-chloro-2,2- difluoroacetyl)phosphoric triamide},
journal = {Acta Crystallographica Section E: Structure Reports Online},
year = {2012},
volume = {68},
number = {10},
month = {October},
issn = {1600-5368},
pages = {3009--3009},
numpages = {0},
keywords = {single-crystal X-ray study; T = 173 K; mean σ(C–C) = 0.005 Å; disorder in main residue; R factor = 0.051; wR factor = 0.122; data-to-parameter ratio = 20.8.},
}
%0 Journal Article
%T N,N- -Dibenzyl-N-- -(2-chloro-2,2- difluoroacetyl)phosphoric triamide
%A Pourayoubi, Mehrdad
%A KEIKHA, MOJTABA
%A Jerry P. Jasinski
%A Amanda C. Keeley
%J Acta Crystallographica Section E: Structure Reports Online
%@ 1600-5368
%D 2012
